1+ {
2+ "ecmofsynthesis" : [
3+ {
4+ "vial_no" : " S-1" ,
5+ "date" : " 01.02.2024" ,
6+ "metal_salt_name" : " FeCl3" ,
7+ "metal_salt_mass" : 16 ,
8+ "metal_salt_mass_unit" : " mg" ,
9+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
10+ "linker_mass" : 16 ,
11+ "linker_mass_unit" : " mg" ,
12+ "solvent" : " DMF" ,
13+ "temperature" : 60 ,
14+ "temperature_unit" : " deg C" ,
15+ "time" : 1 ,
16+ "time_unit" : " day" ,
17+ "place" : " oven" ,
18+ "phase_purity" : true
19+ },
20+ {
21+ "vial_no" : " S-2" ,
22+ "date" : " 01.02.2024" ,
23+ "metal_salt_name" : " FeCl3" ,
24+ "metal_salt_mass" : 16 ,
25+ "metal_salt_mass_unit" : " mg" ,
26+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
27+ "linker_mass" : 16 ,
28+ "linker_mass_unit" : " mg" ,
29+ "solvent" : " DMF" ,
30+ "temperature" : 80 ,
31+ "temperature_unit" : " deg C" ,
32+ "time" : 1 ,
33+ "time_unit" : " day" ,
34+ "place" : " oven" ,
35+ "phase_purity" : true
36+ },
37+ {
38+ "vial_no" : " S-3" ,
39+ "date" : " 01.02.2024" ,
40+ "metal_salt_name" : " FeCl3" ,
41+ "metal_salt_mass" : 16 ,
42+ "metal_salt_mass_unit" : " mg" ,
43+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
44+ "linker_mass" : 16 ,
45+ "linker_mass_unit" : " mg" ,
46+ "solvent" : " DMF" ,
47+ "temperature" : 100 ,
48+ "temperature_unit" : " deg C" ,
49+ "time" : 1 ,
50+ "time_unit" : " day" ,
51+ "place" : " oven" ,
52+ "phase_purity" : true
53+ },
54+ {
55+ "vial_no" : " S-4" ,
56+ "date" : " 01.02.2024" ,
57+ "metal_salt_name" : " FeCl3" ,
58+ "metal_salt_mass" : 16 ,
59+ "metal_salt_mass_unit" : " mg" ,
60+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
61+ "linker_mass" : 16 ,
62+ "linker_mass_unit" : " mg" ,
63+ "solvent" : " Dry DMF" ,
64+ "temperature" : 120 ,
65+ "temperature_unit" : " deg C" ,
66+ "time" : 1 ,
67+ "time_unit" : " day" ,
68+ "place" : " oven" ,
69+ "phase_purity" : true
70+ },
71+ {
72+ "vial_no" : " S-5" ,
73+ "date" : " 01.02.2024" ,
74+ "metal_salt_name" : " FeCl3" ,
75+ "metal_salt_mass" : 16 ,
76+ "metal_salt_mass_unit" : " mg" ,
77+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
78+ "linker_mass" : 16 ,
79+ "linker_mass_unit" : " mg" ,
80+ "solvent" : " DMF" ,
81+ "temperature" : 120 ,
82+ "temperature_unit" : " deg C" ,
83+ "time" : 1 ,
84+ "time_unit" : " day" ,
85+ "place" : " oven" ,
86+ "phase_purity" : true
87+ },
88+ {
89+ "vial_no" : " S-6" ,
90+ "date" : " 01.02.2024" ,
91+ "metal_salt_name" : " FeCl3" ,
92+ "metal_salt_mass" : 16 ,
93+ "metal_salt_mass_unit" : " mg" ,
94+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
95+ "linker_mass" : 16 ,
96+ "linker_mass_unit" : " mg" ,
97+ "solvent" : " DMF" ,
98+ "temperature" : 120 ,
99+ "temperature_unit" : " deg C" ,
100+ "time" : 1 ,
101+ "time_unit" : " hours" ,
102+ "place" : " microwave" ,
103+ "phase_purity" : true
104+ },
105+ {
106+ "vial_no" : " S-7" ,
107+ "date" : " 01.02.2024" ,
108+ "metal_salt_name" : " FeCl3" ,
109+ "metal_salt_mass" : 16 ,
110+ "metal_salt_mass_unit" : " mg" ,
111+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
112+ "linker_mass" : 16 ,
113+ "linker_mass_unit" : " mg" ,
114+ "solvent" : " DMF" ,
115+ "temperature" : 140 ,
116+ "temperature_unit" : " deg C" ,
117+ "time" : 2 ,
118+ "time_unit" : " hours" ,
119+ "place" : " microwave" ,
120+ "phase_purity" : true
121+ },
122+ {
123+ "vial_no" : " S-8" ,
124+ "date" : " 01.02.2024" ,
125+ "metal_salt_name" : " FeCl3" ,
126+ "metal_salt_mass" : 16 ,
127+ "metal_salt_mass_unit" : " mg" ,
128+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
129+ "linker_mass" : 16 ,
130+ "linker_mass_unit" : " mg" ,
131+ "solvent" : " DMF, NaOH" ,
132+ "temperature" : 120 ,
133+ "temperature_unit" : " deg C" ,
134+ "time" : 1 ,
135+ "time_unit" : " day" ,
136+ "place" : " oven" ,
137+ "phase_purity" : false
138+ },
139+ {
140+ "vial_no" : " S-9" ,
141+ "date" : " 01.02.2024" ,
142+ "metal_salt_name" : " FeCl3" ,
143+ "metal_salt_mass" : 16 ,
144+ "metal_salt_mass_unit" : " mg" ,
145+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
146+ "linker_mass" : 16 ,
147+ "linker_mass_unit" : " mg" ,
148+ "solvent" : " DMF, HCI" ,
149+ "temperature" : 120 ,
150+ "temperature_unit" : " deg C" ,
151+ "time" : 1 ,
152+ "time_unit" : " day" ,
153+ "place" : " oven" ,
154+ "phase_purity" : false
155+ },
156+ {
157+ "vial_no" : " S-10" ,
158+ "date" : " 01.02.2024" ,
159+ "metal_salt_name" : " FeCl3�6H2O" ,
160+ "metal_salt_mass" : 27 ,
161+ "metal_salt_mass_unit" : " mg" ,
162+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
163+ "linker_mass" : 16 ,
164+ "linker_mass_unit" : " mg" ,
165+ "solvent" : " DMF" ,
166+ "temperature" : 60 ,
167+ "temperature_unit" : " deg C" ,
168+ "time" : 1 ,
169+ "time_unit" : " day" ,
170+ "place" : " oven" ,
171+ "phase_purity" : false
172+ },
173+ {
174+ "vial_no" : " S-11" ,
175+ "date" : " 01.02.2024" ,
176+ "metal_salt_name" : " FeCl3�6H2O" ,
177+ "metal_salt_mass" : 27 ,
178+ "metal_salt_mass_unit" : " mg" ,
179+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
180+ "linker_mass" : 16 ,
181+ "linker_mass_unit" : " mg" ,
182+ "solvent" : " DMF" ,
183+ "temperature" : 80 ,
184+ "temperature_unit" : " deg C" ,
185+ "time" : 1 ,
186+ "time_unit" : " day" ,
187+ "place" : " oven" ,
188+ "phase_purity" : false
189+ },
190+ {
191+ "vial_no" : " S-12" ,
192+ "date" : " 01.02.2024" ,
193+ "metal_salt_name" : " FeCl3�6H2O" ,
194+ "metal_salt_mass" : 27 ,
195+ "metal_salt_mass_unit" : " mg" ,
196+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
197+ "linker_mass" : 16 ,
198+ "linker_mass_unit" : " mg" ,
199+ "solvent" : " DMF" ,
200+ "temperature" : 100 ,
201+ "temperature_unit" : " deg C" ,
202+ "time" : 1 ,
203+ "time_unit" : " day" ,
204+ "place" : " oven" ,
205+ "phase_purity" : false
206+ },
207+ {
208+ "vial_no" : " S-13" ,
209+ "date" : " 01.02.2024" ,
210+ "metal_salt_name" : " FeCl3�6H2O" ,
211+ "metal_salt_mass" : 27 ,
212+ "metal_salt_mass_unit" : " mg" ,
213+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
214+ "linker_mass" : 16 ,
215+ "linker_mass_unit" : " mg" ,
216+ "solvent" : " DMF" ,
217+ "temperature" : 120 ,
218+ "temperature_unit" : " deg C" ,
219+ "time" : 1 ,
220+ "time_unit" : " day" ,
221+ "place" : " oven" ,
222+ "phase_purity" : false
223+ },
224+ {
225+ "vial_no" : " S-14" ,
226+ "date" : " 01.02.2024" ,
227+ "metal_salt_name" : " FeCl3�6H2O" ,
228+ "metal_salt_mass" : 27 ,
229+ "metal_salt_mass_unit" : " mg" ,
230+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
231+ "linker_mass" : 16 ,
232+ "linker_mass_unit" : " mg" ,
233+ "solvent" : " DMF" ,
234+ "temperature" : 140 ,
235+ "temperature_unit" : " deg C" ,
236+ "time" : 2 ,
237+ "time_unit" : " hours" ,
238+ "place" : " microwave" ,
239+ "phase_purity" : false
240+ },
241+ {
242+ "vial_no" : " S-15" ,
243+ "date" : " 01.02.2024" ,
244+ "metal_salt_name" : " FeCl3�6H2O" ,
245+ "metal_salt_mass" : 27 ,
246+ "metal_salt_mass_unit" : " mg" ,
247+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
248+ "linker_mass" : 16 ,
249+ "linker_mass_unit" : " mg" ,
250+ "solvent" : " DMF, NaOH" ,
251+ "temperature" : 120 ,
252+ "temperature_unit" : " deg C" ,
253+ "time" : 1 ,
254+ "time_unit" : " day" ,
255+ "place" : " oven" ,
256+ "phase_purity" : false
257+ },
258+ {
259+ "vial_no" : " S-16" ,
260+ "date" : " 01.02.2024" ,
261+ "metal_salt_name" : " FeCl3�6H2O" ,
262+ "metal_salt_mass" : 27 ,
263+ "metal_salt_mass_unit" : " mg" ,
264+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
265+ "linker_mass" : 16 ,
266+ "linker_mass_unit" : " mg" ,
267+ "solvent" : " DMF, HCI" ,
268+ "temperature" : 90 ,
269+ "temperature_unit" : " deg C" ,
270+ "time" : 1 ,
271+ "time_unit" : " day" ,
272+ "place" : " oven" ,
273+ "phase_purity" : false
274+ },
275+ {
276+ "vial_no" : " S-17" ,
277+ "date" : " 01.02.2024" ,
278+ "metal_salt_name" : " FeCl3�6H2O" ,
279+ "metal_salt_mass" : 27 ,
280+ "metal_salt_mass_unit" : " mg" ,
281+ "linker_name" : " Benzene-1,4-dicarboxylic acid" ,
282+ "linker_mass" : 16 ,
283+ "linker_mass_unit" : " mg" ,
284+ "solvent" : " DMF, HCI" ,
285+ "temperature" : 120 ,
286+ "temperature_unit" : " deg C" ,
287+ "time" : 1 ,
288+ "time_unit" : " day" ,
289+ "place" : " oven" ,
290+ "phase_purity" : false
291+ }
292+ ]
293+ }
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